Browsing by Author "Asikuzun E., Ozturk O."

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Comparison of theoretical and experimental microhardness of tetrahedral binary Zn1-xErxO semiconductor polycrystalline nanoparticles
(2019-03-01) Asikuzun E., Ozturk O.; Asikuzun, E, Ozturk, O
Zn1−xErxO polycrystalline nanoparticles with various compositions (x=0.01,0.02,0.03,0.04,0.05, and 0.10)were prepared using sol–gel techniques, for which zinc acetate dihydrate and erbium 2–4 pentanedionate are used as precursors. Nanoparticles were pressed under a pressure of 4 tons for 5 min into disk-shaped compacts with 2 mm thicknesses and 10 mm diameters. The pressed samples were annealed at 400 °C for 30 min. X-ray diffraction (XRD), scanning electron microscopy (SEM), and Vickers microhardness analyses of the produced Er-doped ZnO bulk nanomaterials were performed. Specifically, in this study we focused on the analysis of their mechanical properties. Undoped and Er-doped bulk samples were investigated according to Meyer's law; the proportional sample resistance (PSR), elastic/plastic deformation (EPD), and indentation-induced cracking (IIC) models; and the Hays–Kendal (HK) approach. As a result, the IIC model was more suitable to determine the micromechanical properties and the reverse indentation size effect (RISE) behavior of Er-doped ZnO semiconductors.
Theoretical and experimental approaches to measuring mechanical properties of Zn1−xCoxO binary tetrahedral bulk semiconductors
(2018-05-01) Asikuzun E., Ozturk O.; Asikuzun, E, Ozturk, O
We prepared a Zn 1 - xCo xO system as polycrystalline nanoparticles with various compositions (x=0.01,0.02,0.03,0.04,0.05,and0.10) using sol–gel techniques and use zinc acetate dihydrate and cobalt acetate tetrahydrate as precursors. Nanoparticles were pressed under a pressure of 4 tons for 5 min into 2 mm thick disk shaped compacts 10 mm in diameter, which were then annealed at 500 °C for 30 min under a 5B Ar atmoshpere. We carried out X-ray diffraction, scanning electron microscopy, and Vickers microhardness analyses of Co doped Zno -based nano bulk materials in detail, focusing especially on theoretical and experimental mechanical analyses. We found that calculated values were higher than the Vickers microhardness experimental results. Doping ZnO with Co did not lead to significant changes in the a and c axes. The calculated hardness values are larger than those from the experiments. Acoording to the SEM and EDS images grain size decreases as Co doping increases and the amount of Zn decreases with Co doping, respectively.